ANGGA PRATAMA ERDIYAN, 050610264 (2011) ANALISIS NATRIUM BENZOAT SEBAGAI BAHAN PENGAWET DALAM SEDIAAN NATA DE COCO DENGAN METODE KLT-DENSITOMETRI. Skripsi thesis, UNIVERSITAS AIRLANGGA.
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Abstract
Sodium benzoate as a preservative in Nata de coco’s sample was determined by TLC-densitrometry . The chromatogram was performed on silica gel 60F254 plates with a mixture Toluen : Aseton : HCOOH (6:3:1) v/v as the mobile phase. Retardation factor (Rf) of benzoic acid was obtained 0,57. The chromatographic zones corresponding to the Benzoic acid spot were scanned using densitometric method at λ = 227 nm. The relationship between the peak area and the concentration of benzoic acid was evaluated by linier regression analysis. Correlation coefficients being r = 0,9972 (Vxo=1,92%). Sample was spotted using 2 μl capillary pipette. Mean of recovery values was 95,07% and RSD values was 7,25%. The proposed method was applied for sodium benzoate determination in Nata de coco’s sample. The result showed that sodium benzoate concentration in nata de coco sample was 0,08 - 0,1 mg/g. So that, amount of sodium benzoate in sample Nata de coco was fulfill The regulation stated in The Rule Menkes RI No. 722/Menkes/Per/IX/1988
Item Type: | Thesis (Skripsi) | ||||||
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Additional Information: | KKB KK-2 FF.KF.21/13 Erd a | ||||||
Uncontrolled Keywords: | BENZOID ACID, NATA DE COCO, TLC- DENSITOMETRY | ||||||
Subjects: | R Medicine > RM Therapeutics. Pharmacology | ||||||
Divisions: | 05. Fakultas Farmasi > Kimia Farmasi | ||||||
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Depositing User: | mat sjafi'i | ||||||
Date Deposited: | 13 Feb 2013 12:00 | ||||||
Last Modified: | 01 Sep 2016 05:08 | ||||||
URI: | http://repository.unair.ac.id/id/eprint/9075 | ||||||
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