AGUSTIN DIAN PUSPITA, 050911194 (2013) SINTESIS 6-(PIPERIDIN-1-ILMETIL)PINOSTROBIN MELALUI REAKSI MANNICH DARI MATERIAL AWAL PINOSTROBIN. Skripsi thesis, UNIVERSITAS AIRLANGGA.
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Abstract
The aim of this study was to synthesize 6-(piperidine-1- ylmetyl)pinostrobin as a target compound by Mannich reaction. Piperidine was reacted with formalin to form iminium salt as an intermediate product. The target compound was synthesized by reacting the iminium salt with pinostrobin in three different reaction times, that are 1 hour, 2 hours, and 3 hours, respectively. The structure of 6-(piperidine-1-ylmethyl)pinostrobin was confirmed by IR and 1H-NMR spectroscopy. The highest percentage yield of 12% was obtained over reaction time of 3 hours.
| Item Type: | Thesis (Skripsi) | ||||||
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| Additional Information: | KKB KK-2 FF.KF 70/13 Pus s | ||||||
| Uncontrolled Keywords: | MANNICH REACTION | ||||||
| Subjects: | Q Science > Q Science (General) > Q1-390 Science (General) Q Science > QD Chemistry > QD71-142 Analytical chemistry |
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| Divisions: | 05. Fakultas Farmasi > Kimia Farmasi | ||||||
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| Depositing User: | shiefti dyah alyusi | ||||||
| Date Deposited: | 09 Jan 2014 12:00 | ||||||
| Last Modified: | 11 Aug 2016 08:41 | ||||||
| URI: | http://repository.unair.ac.id/id/eprint/9762 | ||||||
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